Preface ........................................................ ix
Introduction ................................................... xi
Selected Monographs and Reviews ................................. 1
Acrylonitrile ................................................... 9
Allyl Ethylsulfone ............................................. 16
Allyltributylstannane .......................................... 19
Allyltriphenylstannane ......................................... 29
4,4'-Azobis(4-cyanopentanoic acid) ............................. 30
l,l'-Azobis-1-cyclohexanenitrile ............................... 32
2,2'-Azobis(2,4-dimethyl-4-methoxyvaleronitrile) ............... 32
2,2'-Azobis[2-(2-imidazolin-2-yl)-propanel Dihydrochloride ..... 34
Azobisisobutyronitrile ......................................... 36
2,2'-Azobis(2-methylpropanimidamide)Dihydrochloride ............ 37
Benzeneselenol ................................................. 39
Benzenesulfonyl Azide .......................................... 45
l,2-Benziodoxol-3(1H)-one Derivatives .......................... 48
4,5-Bis(1,1-dimethylethyl)-6-ethoxy-2,2-dimethyl-3,
7-dioxa-4-aza-6-phosphanonanoic Acid 6-oxide ................... 51
Bis(dimethylglyoximato)(methyl)(pyridine)cobalt(III) ........... 53
Bis(ethoxythiocarbonyl)sulfide ................................. 58
Bis[(1R,2S,5R)-menthyl](phenyl)tin Hydride ..................... 60
Bis[4-(tridecafluorohexyl)phenyl] Diselenide ................... 61
Bis(trimethylstannyl) Benzopinacolate .......................... 63
Bromine Azide .................................................. 65
Bromine Trifluoride ............................................ 66
(1-Bromoethenyl)chlorodimethylsilane ........................... 72
(Bromomethyl)chlorodimethylsilane .............................. 73
N-Bromosuccinimide ............................................. 79
Bromotrichloromethane .......................................... 89
t-Butyl Hydroperoxide .......................................... 92
t-Butyl Hypochlorite .......................................... 112
t-Butyl Hypoiodite ............................................ 117
t-Butyl Isocyanide ............................................ 119
N-t-Butyl-1-diethylphosphono-2,2-dimethylpropy1 Nitroxide ..... 129
Carbon Monoxide ............................................... 133
Carbon Tetrabromide ........................................... 148
Carbon Tetraiodide ............................................ 150
Catecholborane ................................................ 152
Cerium(IV) Ammonium Nitrate ................................... 159
Chlorobis(dimethylglyoximato)(pyridine)cobalt(III) ............ 166
N-Chloro-N-cyclohexylbenzenesulfonamide ....................... 174
4-(4-Chlorophenyl)-3-hydroxy-2(3H)thiazolethione .............. 175
Chromium(II) Acetate .......................................... 179
Chromium(II) Chloride ......................................... 183
Cobalt Salen Complexes ........................................ 192
Cobalt Salophen Complexes ..................................... 194
Copper(II) Acetate ............................................ 195
1,4-Cyclohexadiene ............................................ 202
Decacarbonyldimanganese ....................................... 205
(Diacetoxyiodo)benzene ........................................ 208
Dibenzoyl Peroxide ............................................ 217
Di-t-butyl Hyponitrite ........................................ 228
1,1-Di-t-buty1 Peroxide ....................................... 232
2,2-Di(t-butylperoxy)butane ................................... 238
Di-t-butyl Peroxyoxalate ...................................... 239
N,N-Dichlorobenzenesulfonamide ................................ 242
2,3-Dichloro-5,6-dicyano-1,4-benzoquinone ..................... 244
Dilauroyl Peroxide ............................................ 256
1,4:5,8-Dimethano-1,2,3,4,5,6,7,8-octahydro-9,10-
dimethoxyanthracenium Hexachloroantimonate .................... 265
(2,6-Dimethoxy-1-methy1-2,5-cyclohexadien-1-yl)
(1,1-dimethylethyl)dimethylsilane ............................. 267
[2-(Dimethylamino)methyl]phenyl Dimethyltin Hydride ........... 269
2,2-Dimethyl-5-[3-(diphenylstannyl)propyl]-1,3-dioxolan-
4-one ......................................................... 271
Dimethyl Disulfide ............................................ 272
5,5-Dimethyl-1-(phenylmethyl)-3-pyrazolidinone ................ 275
Dimethyl[3-(l-pyrenyl)propyl]stannane ......................... 278
Diphenyl Diselenide ........................................... 279
Diphenyl Disulfide ............................................ 285
Diphenyl Disulfone ............................................ 288
Diphenyl Ditelluride .......................................... 290
Diphenyl [2-(4-pyridyl)ethyl]tin hydride ...................... 291
2,2'-Dipyridyl Disulfide N,N'-Dioxide ......................... 292
t-Dodecanethiol ............................................... 296
Ethanesulfonyl Azide .......................................... 299
Ethyl Difluoroiodoacetate ..................................... 300
Galvinoxyl .................................................... 303
Hexabutyldistannane ........................................... 305
Hexamethyldistannane .......................................... 307
Hydrogen Bromide .............................................. 309
Hydrogen Selenide ............................................. 311
N-Hydroxyphthalimide .......................................... 315
N-Hydroxypyridine-2-thione .................................... 321
Hypophosphorous Acid .......................................... 331
Indium ........................................................ 337
Iodine Azide .................................................. 353
Iodine-Nitrogen Tetroxide ..................................... 358
2'-Iodobiphenyl-2-thiol Dimethylaluminum Complex .............. 360
Iodoform ...................................................... 361
Iodosylbenzene ................................................ 365
1-Iodo-2-(2,2,2-triethoxyethyl)benzene ........................ 375
Iron, Bis(pyridine)bis(2-pyridinecarboxylato-N1,O2) ........... 376
Iron(III) Chloride ............................................ 380
Lead(IV) Acetate .............................................. 389
Lead(IV) Acetate-Copper(II) Acetate ........................... 396
Lead(IV) Acetate-Iodine ....................................... 397
Lithium 4,4'-Di-t-butylbiphenylide ............................ 399
Lithium 1-(Dimethylamino)naphthalenide ........................ 403
Lithium Naphthalenide ......................................... 404
Manganese(III) Acetate ........................................ 407
Manganese(III) Acetate-Copper(II) Acetate ..................... 409
Manganese(III) Acetylacetonate ................................ 411
Mercury(II) Oxide-Bromine ..................................... 412
Mercury(II) Oxide-Iodine ...................................... 413
Methyl Acrylate ............................................... 415
1-Methyl-2-azaadamantane N-Oxyl ............................... 421
N-Methylcarbazole ............................................. 422
S-Methyl N-methyl-N-hydroxydithiocarbamate .................... 424
N-Methylquinolinium Hexafluorophosphate ....................... 426
1-[(Methyltelluro)ethyl]benzene ............................... 428
Methyl Thioglycolate .......................................... 429
Naphthalene-1,8-diyl Bis(diphenylmethylium) Perchlorate ....... 433
4-Nitrobenzenesulfenyl Chloride ............................... 434
o-Nitrobenzenesulfonylhydrazide ............................... 436
Nitroethylene ................................................. 438
Nitrosobenzene ................................................ 442
Nitrosyl Chloride ............................................. 452
5-(l-Oxido-2-pyridinyl)-1,1,3,3-tetramethylthiouronium
Hexafluorophosphate (HOTT) .................................... 455
4-Pentyne-1-thiol ............................................. 457
Peroxyacetyl Nitrate .......................................... 458
Phenyl Chlorothionocarbonate .................................. 460
Phenyliodine(III) Dichloride .................................. 462
Phenylsulfonylethylene ........................................ 465
Phosphinic Acid, Alkyl Esters ................................. 469
Polymethylhydrosiloxane (PMHS) ................................ 473
Potassium 0-ethyl Xanthate .................................... 478
Potassium Ferricyanide ........................................ 488
3-Pyridinesulfonyl Azide ...................................... 492
2-Pyridinethiol ............................................... 493
Samarium(II) Iodide ........................................... 499
Se-Phenyl p-tolueneselenosulfonate ............................ 509
Sodium Anthracenide ........................................... 512
Sodium Bis(dimethylglyoximato)(pyridine)cobaltate ............. 513
Sodium Hypophosphite .......................................... 515
Sodium Naphthalenide .......................................... 516
Sulfuryl Chloride ............................................. 519
2,2,6,6-Tetramethylpiperidin-1-oxyl ........................... 525
Tetraphenyldiphosphine ........................................ 531
1,1,2,2-Tetraphenyldisilane ................................... 535
Tetrathiafulvalene ............................................ 539
1,1'-Thiocarbonylbis(1H-benzotriazole) ........................ 544
1,1'-Thiocarbonyldiimidazole .................................. 545
Thionocarbonates .............................................. 551
Thiophenol .................................................... 553
Thiophosgene .................................................. 563
Titanium(III) Chloride ........................................ 567
O-p-Tolyl Chlorothioformate ................................... 570
Tri(t-butoxy)silanethiol ...................................... 571
Tri-n-butyl(iodoacetoxy)stannane .............................. 574
Tri-n-butylstannane ........................................... 575
Triethylborane ................................................ 585
Triethylsilane ................................................ 601
m-Trifluoromethylbenzoyl Chloride ............................. 609
α,α,α-Trifluorotoluene ........................................ 611
Triisopropylsilanethiol ....................................... 614
Trimethylstannane ............................................. 618
Triphenylbismuthine ........................................... 619
Triphenylsilane ............................................... 620
Triphenylstannane ............................................. 626
Tris(2-perfluorohexylethyl)tin Hydride ........................ 629
Tris(phenylthio)phosphine ..................................... 632
Tris(trimethylsilyl)silane .................................... 633
Trityl Thionitrite ............................................ 640
Vanadyl Trichloride ........................................... 643
Vitamin В12 ................................................... 644
Xenon(II) Fluoride ............................................ 649
Ytterbium(II) Chloride......................................... 651
Ytterbium(III) Trifluoromethanesulfonate & Ytterbium(III)
Trifluoromethanesulfonate Hydrate ............................. 652
List of Contributors .......................................... 659
Reagent Formula Index ......................................... 673
Subject Index ................................................. 677
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